MS Report from Instrument: LCMS-03 File ..018\\20180828\\20180828 1\\CPK2018-828-18037.D Tgt Mass (CHM): Injection Date : 28 Aug 18 6:28 pm +0800 Seq. Line : 62 Sample Name : CPK2018-828-18037 Location : P2-C-08 Acq. Operator : SYSTEM Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\LCMS03\\Data\\2018\\20180828\\20180828 1\\1-POS-3MIN.M Analysis Method : D:\\LCMS03\\Data\\2018\\20180828\\20180828 1\\1-POS-3MIN.M Catalog No : HY-12750 Batch#18037 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C DAD1 A, Sig=214,4 Ref=off1.5831.302mAU6004001.8891.928200000.5 ELS1 A, ELSD SignalmV20151000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 708000006000002000000.0624000001.51.60922.5min1.66612.0271.522.5min00.511.5 Ion 516.5, MSD1 516.5,Target Mass 515.5 +H Positive, EIC=516.2:517.2600000400000200000000.511.51.59622.5min1.64922.5min Integration Results for DAD1 A, Sig=214,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.30 0.03 0.72 0.36 0.07 233 1.58 0.02 962.05 738.98 99.59 516 1.89 0.02 1.30 1.10 0.13 233 1.93 0.03 1.06 0.60 0.11 233 2.03 0.03 0.91 0.52 0.09 233 Integration Results for ELS1 A, ELSD Signal RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.67 0.05 59.35 17.40 100.00 516 Integration Results for MSD1 TIC, MS File RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.06 0.04 240973.58 98694.63 6.44 279 1.61 0.06 3499401.25 876176.81 93.56 516LCMS-03 8/29/2018 7:44:17 AM SYSTEMPage1 of3MS Report from Instrument: LCMS-03Ret. Time: 0.06 <<<< POSITIVE SPECTRA >>>> ES-API Positive152.1279.1294.1199.1260.0259.0277.1293.9310.3338.160005000102.340003000200010000100122.1141.1158.1177.2202.1236.3391.3200300400500600700800900m/zRet. Time: 1.61 ES-API Positive1400001200001000008000060000233.140000200000100200300400500600700800900m/z518.2517.2516.2LCMS-03 8/29/2018 7:44:17 AM SYSTEMPage2 of3MS Report from Instrument: LCMS-03 *** End of Report ***LCMS-03 8/29/2018 7:44:17 AM SYSTEMPage3 of3