Data File D:\\AGLIENT 1260\\DATA\\20151117\\20151117 2015-11-17 08-55-00\\BIZ2015-N17-WJ6.DSample Name: BIZ2015-N17-WJ6=====================================================================Acq. Operator : Yang Qian(LCMS-02) Seq. Line : 49Acq. Instrument : HY-LCMS-02 Location : P1-A-05Injection Date : 11/17/2015 1:15:17 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20151117\\20151117 2015-11-17 08-55-00\\100-1000MS+3MIN- 1.5_(0.02%FA)-BD.MLast changed : 11/17/2015 8:55:00 AM by Yang Qian(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\DATA\\20151110\\20151110 2015-11-10 11-24-47\\100-1000MS+3MIN- 1.5_(0.02%FA)-BD.M (Sequence Method)Last changed : 11/17/2015 4:14:37 PM by Yang Qian(LCMS-02) (modified after loading)Method Info : Postive,MS:100-1000,Column ID:A-RP-132,40℃ Catalog No : HY-19323 Batch#18635 A-RP-134 Additional Info : Peak(s) manually integrated DAD1 C, Sig=254,4 Ref=off (D:\\AGLIENT 1260\\DATA\\20151117\\20151117 2015-11-17 08-55-00\\BIZ2015-N17-WJ6.D) 1.628mAU12001000800600400 2.418 1.89820000.51 1.529 2.027 2.7561.522.53min ===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier : 1.0000Dilution : 1.0000Do not use Multiplier & Dilution Factor with ISTDs Signal 1: DAD1 C, Sig=254,4 Ref=off Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 1.529 MM 0.0472 6.08605 2.14696 0.1536 2 1.628 MM 0.0437 3935.28638 1501.09680 99.3270 3 1.898 MM 0.0391 1.89061 8.04879e-1 0.0477 4 2.027 MM 0.0398 1.27747 5.35091e-1 0.0322 5 2.418 MM 0.1059 12.24643 1.92795 0.3091 6 2.756 MM 0.1078 5.16475 7.98762e-1 0.1304 Totals : 3961.95168 1507.31045 ===================================================================== *** End of Report ***HY-LCMS-02 11/17/2015 4:14:39 PM Yang Qian(LCMS-02)Page 1 of 1
Data File D:\\AGLIENT 1260\\DATA\\20151117\\20151117 2015-11-17 08-55-00\\BIZ2015-N17-WJ6.DSample Name: BIZ2015-N17-WJ6=====================================================================Acq. Operator : Yang Qian(LCMS-02) Seq. Line : 49Acq. Instrument : HY-LCMS-02 Location : P1-A-05Injection Date : 11/17/2015 1:15:17 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20151117\\20151117 2015-11-17 08-55-00\\100-1000MS+3MIN- 1.5_(0.02%FA)-BD.MLast changed : 11/17/2015 8:55:00 AM by Yang Qian(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\DATA\\20151110\\20151110 2015-11-10 11-24-47\\100-1000MS+3MIN- 1.5_(0.02%FA)-BD.M (Sequence Method)Last changed : 11/17/2015 4:15:24 PM by Yang Qian(LCMS-02) (modified after loading)Method Info : Postive,MS:100-1000,Column ID:A-RP-132,40℃ Catalog No : HY-19323 Batch#18635 A-RP-134 Additional Info : Peak(s) manually integrated MSD1 TIC, MS File (D:\\AGLIENT 1260\\DATA\\20151117\\20151117 2015-11-17 08-55-00\\BIZ2015-N17-WJ6.D) ES-API, Pos, Scan 1.63310000008000006000004000002000000.511.522.53min HY-LCMS-02 11/17/2015 4:15:25 PM Yang Qian(LCMS-02)Page 1 of 2
Data File D:\\AGLIENT 1260\\DATA\\20151117\\20151117 2015-11-17 08-55-00\\BIZ2015-N17-WJ6.DSample Name: BIZ2015-N17-WJ6MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts. Reportable Ion Abundance: > 10%. Retention Mol. WeightTime (MS) MS Area or Ion 1.633 4484221 414.20 I 413.20 I 207.10 I 130.20 I*MSD1 SPC, time=1.616:1.653 of D:\\AGLIENT 1260\\DATA\\20151117\\20151117 2015-11-17 08-55-00\\BIZ2015-N17-WJ6.D ES-API, 100806040 413.2Max: 478123 130.2 207.1200100 415.2200300400500600700800m/z *** End of Report ***HY-LCMS-02 11/17/2015 4:15:25 PM Yang Qian(LCMS-02)Page 2 of 2